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不同风味接装纸中特征成分的衰减行为研究

107    2024-05-24

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作者:冯懂懂1, 冯衍闯2, 张震1, 倪和朋1, 梁淼2, 黄珂2, 朱鑫超2, 张钱双燕1, 谭淞彦1, 张峻松2

作者单位:1. 红塔烟草(集团)有限责任公司玉溪卷烟厂,云南 玉溪 653110;
2. 郑州轻工业大学食品与生物工程学院,河南 郑州 450001


关键词:风味接装纸;特征成分;衰减;动力学


摘要:

为研究风味接装纸中特征成分的衰减行为,以纽甜、薄荷醇和苹果酸为研究对象,对不同储存时间下各风味接装纸中的特征成分进行提取和检测,并采用零级、一级和Higuchi动力学模型对其衰减曲线进行拟合,获得合适的动力学模型及参数。结果表明:风味接装纸中薄荷醇的衰减率最高,纽甜次之,苹果酸最不易衰减;风味接装纸中纽甜添加量为326.53 μg/g的衰减更符合Higuchi动力学模型Q=0.6269t1/2,薄荷醇添加量为6244.52 μg/g的衰减更符合Higuchi动力学模型Q=5.0265t1/2,苹果酸添加量为143.92 μg/g的衰减更符合一级动力学模型Q=1.1167(1–e–0.0306t)。该方法可较好地预测风味接装纸中特征成分的衰减行为,为风味物质在接装纸中的应用提供基础数据支撑。


Study on attenuation behavior of characteristic components in different flavor tipping papers
FENG Dongdong1, FENG Yanchuang2, ZHANG Zhen1, NI Hepeng1, LIANG Miao2, HUANG Ke2, ZHU Xinchao2, ZHANG Qianshuangyan1, TAN Songyan1, ZHANG Junsong2
1. Yuxi Cigarette Factory, Hongta Tobacco (Group) Co., Ltd., Yuxi 653110, China;
2. School of Food and Bioengineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China
Abstract: In order to study the attenuation behavior of characteristic components in flavor tipping papers. Taking neotame, menthol and malic acid as the research objects, the characteristic components of each flavor tipping paper under different storage time were extracted and detected. The attenuation curve was fitted by zero order, first order and Higuchi dynamic models, and the appropriate dynamic model and parameters were obtained. The results showed that the attenuation rate of menthol in flavor tipping papers was the highest, followed by neotame and malic acid. The attenuation of neotame, which’s addition amount in flavor tipping paper was 326.53 μg/g, was more in line with Higuchi kinetic model (Q=0.6269t1/2). The attenuation of menthol, which’s addition amount in flavor tipping paper was 6244.52 μg/g, was more in line with Higuchi kinetic model (Q=5.0265t1/2). The attenuation of malic acid, which’s addition amount in flavor tipping paper was 143.92 μg/g, was more in line with first order kinetic model (Q=1.1167(1–e–0.0306t)). This method can predict the attenuation behavior of characteristic components in flavor tipping paper, and provide basic data support for the application of flavor substances in tipping paper.
Keywords: flavor tipping paper;characteristic component;attenuation;kinetics
2024, 50(5):79-85,121  收稿日期: 2021-10-29;收到修改稿日期: 2022-01-03
基金项目: 红塔烟草(集团)有限责任公司科技项目(HTYX-2020-0252 109791)
作者简介: 冯懂懂(1989-),男,云南玉溪市人,工程师,硕士,主要从事卷烟质量管控与烟草化学方面研究。
参考文献
"[1] 吴秉宇, 费婷, 罗辰, 等. 细支卷烟不同加香方式香味成分的转移行为[J]. 烟草科技, 2021, 54(1): 24-31.
WU B Y, FEI T, LUO C, et al. Smoke transfer of aroma components in slim cigarettes flavored by different methods[J]. Tobacco Science & Technology, 2021, 54(1): 24-31.
[2] 孙兰茜, 周维, 黎洪利, 等. 珠兰精油挥发性成分及其加香方式对卷烟评吸效果的影响[J]. 贵州农业科学, 2020, 48(10): 127-130.
SUN L X, ZHOU W, LI H L, et al. Effect of volatile components in chloranthus spicatus essential oil and its flavor adding pattern on smoking evaluation of cigarette[J]. Guizhou Agricultural Sciences, 2020, 48(10): 127-130.
[3] 徐秀娟, 王甜, 何保江, 等. 滁菊挥发油的成分分析及其在卷烟中的应用[J]. 天然产物研究与开发, 2015, 27(9): 1532-1538.
XU X J, WANG T, HE B J, ey al. Chemical components of chrysanthemum morifolium( ramat)tzvel. cv. chuju volatile oil and its applications in cigarette flavoring[J]. Natural Product Research and Development, 2015, 27(9): 1532-1538.
[4] 邱光明, 王毅, 李朝荣, 等. 黄皮提取物在卷烟中的应用[J]. 香料香精化妆品, 2020(4): 26-30.
QIU G M, WANG Y, LI C R, et al. The application of extract of clausena lansium(lour.)skeels in cigarette[J]. Flavour Fragrance Cosmetics, 2020(4): 26-30.
[5] 杨伟平, 姬凌波, 霍现宽, 等. 铁观音茶香提取物的制备、分析及其在卷烟中的应用[J]. 香料香精化妆品, 2019(6): 14-20.
YANG W P, JIL B, HUO X K, et al. The preparation, analysis of aroma extracts obtained from Tie Guanyin tea and its application in cigarettes[J]. Flavour Fragrance Cosmetics, 2019(6): 14-20.
[6] 陈淑英, 叶荣飞. 微胶囊技术在卷烟设计中的研究进展[J]. 安徽农业科学, 2013, 41(32): 12713-12715.
CHEN S Y, YE R F. Research status of microencapsulation technology in cigarette design[J]. Journal of Anhui Agricultural Sciences, 2013, 41(32): 12713-12715.
[7] 张建铎, 杨文武, 向海英, 等. 超高效液相色谱-串联质谱测定卷烟爆珠中7种着色剂[J]. 中国测试, 2019, 45(6): 77-80.
YANG J D, YANG W W, XIANG H Y, et al. Determination of seven colorants in cigarette breakable capsule by ultra-high performance liquid chromatograph-tandem mass spectrometry[J]. China Measurement & Test, 2019, 45(6): 77-80.
[8] 李响丽, 张凤梅, 范多青, 等. 高效液相色谱-二极管阵列法同时测定卷烟爆珠壁材中10种水溶性合成着色剂[J]. 中国测试, 2021, 47(3): 76-81.
LI X L, ZHANG F M, FAN D Q, et al. Simultaneous determination of 10 water-soluble synthetic colorants in cigarette bead wall materials by high performance liquid chromatography-diode array[J]. China Measurement & Test, 2021, 47(3): 76-81.
[9] 赵荣艳, 杨江涛, 王安. 新型烟用接装纸及其应用现状简述[J]. 纸和造纸, 2021, 40(4): 26-31.
ZHAO R Y, YANG J T, WANG A. Application status of new tipping paper for cigarettes[J]. Paper and Paper Making, 2021, 40(4): 26-31.
[10] 付强, 李国政, 林奕云, 等. UPLC-MS/MS法测定胶基型嚼烟中13种甜味剂[J]. 烟草科技, 2019, 52(12): 31-38.
FU Q, LI G Z, LIN Y Y, et al. Determination of thirteen sweeteners in gum-based chewing tobacco with UPLC-MS/MS method[J]. Tobacco Science & Technology, 2019, 52(12): 31-38.
[11] 王紫燕, 韩敬美, 袁大林, 等. 气相色谱-质谱联用法测定加热卷烟烟草材料中8种凉味剂[J]. 烟草科技, 2020, 53(6): 57-63.
WANG Z Y, HAN J M, YUAN D L, et al. Determination of eight cooling agents in tobacco materials for heated tobacco products by gas chromatography-mass spectrometry[J]. Tobacco Science & Technology, 2020, 53(6): 57-63.
[12] 邱宝平, 王政, 刘晓旭, 等. 响应面法对烟草中非挥发性有机酸含量测定的优化[J]. 湖北农业科学, 2014, 53(15): 3629-3633.
QIU B P, WANG Z, LIU X X, et al. Optimizing the determination of non-volatile organic acids in tobacco with response surface methodology[J]. Hubei Agricultural Sciences, 2014, 53(15): 3629-3633.
[13] 杨明, 杨荣平. 中药缓释剂的药代动力学研究[J]. 世界科学技术-中医药现代化, 2004(3): 19-21.
YANG M, YANG R P. A Study on pharmacokinetics of slow releasing drugs of traditional chinese medicine[J]. Modernization of Traditional Chinese Medicine and Materia Medica-World Science and Technology, 2004(3): 19-21.
[14] 吴建煌, 丁州, 雷青, 等. 利福平-聚乳酸-羟基乙酸-磷酸钙骨水泥缓释复合体的实验研究[J]. 中南大学学报(医学版), 2016, 41(9): 946-954.
WU J H, DING Z, LEI Q, et al. An experimental study on a slow-release complex with rifampicin-polylactic-co-glycolic acid-calcium phosphate cement[J]. Journal of Central South University :Medical Science, 2016, 41(9): 946-954.
[15] 张海波, 蒋建新, 高宏, 等. 松香基聚丙烯酰胺水凝胶的药物释放性能及其动力学研究[J]. 林产化学与工业, 2018, 38(3): 25-32.
ZHANG H B, JIANG J X, GAO H, et al. Drug release and kinetics properties of rosin-based polyacrylamide hydrogels[J]. Chemistry and Industry of Forest Products, 2018, 38(3): 25-32.
[16] IFTIME M M, DOBRECI D L, IRIMICIUC S A, et al. A theoretical mathematical model for assessing diclofenac release from chitosan-based formulations[J]. Drug Delivery, 2020, 27(1): 1125-1133.
[17] 金青, 齐娟. 两种苦参碱缓释微粒的释放动力学研究[J]. 青岛科技大学学报(自然科学版), 2019, 40(1): 33-37.
JIN Q, QI J. Study on the release kinetics of two kinds of matrine sustained-release microcapsules[J]. Journal of Qingdao University of Science and Technology:Natural Science Edition, 2019, 40(1): 33-37.
[18] 岳龙凯, 王伯仁, 黄庆海, 等. 长期施肥红壤及其有机无机复合体非交换性钾释放动力学[J]. 中国农业科学, 2015, 48(23): 4748-4758.
YUE L K, WANG B R, HUANG Q H, et al. The release kinetics of non-exchangeable potassium in red soil and its organo-mineral complex of long-term fertilizer experiments[J]. Scientia Agricultura Sinica, 2015, 48(23): 4748-4758.
[19] 余丽丽, 尤静, 姚琳, 等. 盐酸小檗碱β-环糊精聚合物微球的制备和释药性能研究[J]. 化工新型材料, 2013, 41(6): 53-55.
YU L L, YOU J, YAO L, et al. Synthesis of berberine hydrochloride encapsulated into β-cyclodextrin polymer microspheres and its behavior of drug release[J]. New Chemical Materials, 2013, 41(6): 53-55.
[20] 冯丹, 齐孝蕾, 郝健, 等. 薄荷醇作为临时固型材料在文物保护中的应用[J]. 文物保护与考古科学, 2020, 32(2): 112-117.
FENG D, QI X L, HAO J, et al. Application of menthol as a temporary consolidant in cultural relic conservation[J]. Sciences of Conservation and Archaeology, 2020, 32(2): 112-117.
[21] 杜淑霞, 林楠. 纽甜的稳定性研究[J]. 中国调味品, 2012, 37(2): 14-16.
DU S X, LI N. Study on stability of NEOTAME[J]. China Condiment, 2012, 37(2): 14-16.